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Abstract

The study was focused on the red dragon fruit (Hylocerens polyrhizus) peel which can be used as a source of pectin .The physicochemical properties were studied moisture, protein, fat, ash, total soluble solid TSS, pH and titratable acidity TA .Using three different concentration of ammonium oxalate 0.5 ,1 ,2 gm. At pH 4.9, temperature 90 ?C, time 90 min to extract pectin. Highest yield with about 0.5 gm. Concentration ammonium oxalate was 26.64% following 23.75%, 15.88% yields at concentration 1 and 2 gm. ammonium oxalate .There were significant differences in yields at (p< 0.05). Characterization of the extracted pectin in terms of equivalent weight, methoxyl  content, degree of esterification, an hydrouronic acid AUA, Fourier-transform infrared spectroscopy FTIR, viscosity, setting times were studied. Based on the value of methoxyl content 2.54% and degree esterification pectin can be categorized as low methoxyl.

Keywords

Ammonium oxalate Dragon fruit peel Extraction Pectin

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How to Cite
Hashim, A. Z. . (2018). Extraction and Characterization of Pectin from Dragon Fruit (Hylocerens polyrhizus) Peel Using Different Concentration of Ammonium Oxalate. Basrah Journal of Agricultural Sciences, 31(1), 12–19. https://doi.org/10.37077/25200860.2018.70
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References

  1. A.O.A.C. (1990). Official methods of analysis. 15th ed., Washington, D. C.: 771pp.
  2. Bartley, J.M. & Knee, M. (1981). Composition and metabolism of cell wall polysaccharides in ripening fruits. Pp: 133-148. In: Friend, J. & Rhodes, M.J.C. (Eds.). Recent Advances in the Biochemistry of Fruits and Vegetables. New York. Academic Press: 275pp.
  3. Cardoso, S. M.; Coimbra, M.A. & Lopesd Silva, J.A. (2003). Temperature dependence of the formation and melting of pectin Ca2+ networks: Archeological study. Food Hydrocolloids, 17: 801-807.
  4. Chakraborty, A. & Ra, S. (2011). Development of a process for the extraction of pectin from citrus fruit wastes viz. Lime Peel, Spent guava extract, Apple pomace etc. International Journal of Food Safety, 13: 391-397.
  5. Chatjigakis, A.K.; Pappas, C.; Proxenia, N.; Kalantzi, O.; Rodis, P. & Polissiou, M. (1998). FT-IR spectroscopic determination of the degree of esterification of cell wall pectins from stored peaches and correlation to textural changes. Carbohydrate Polymers, 37(4): 395- 408.
  6. F.C.C.: Food Chemical Codex (2004). Pectins. 5th ed. National Academy of Science: Washington, D.C.: 998pp. (Cited from Rahmati et al., 2015).
  7. Gannasin, S.P.; Ramakrishnan, Y.; Adzahan, N.M. & Muhammad, K. (2012). Functional and preliminary characterisation of hydrocolloid from tamarillo (Solanum betaceum Cav.) puree. Molecules, 17(6): 6869-6885.
  8. Haber, W.A. (1983). Hylocereus costaricensis (Pitahaya silvestre), wild pitahaya. Pp:
  9. -253 In Janzen, D.H. (Ed.). Costarcan natural history. Chicago. Univ. Chicago Press: 823pp. (Cited from Rahmati et al., 2015).
  10. Hamapitour, M.S.; Majidi, S.M.; Abdi, M. & Nia, F. (2004). Potential for industrial utilization of citrus by products. CHISA 16th Int. Congress of Chemical and Process Engineering 62: 215-223.
  11. Hoa, T.T.; Clark, C.J.; Waddell, B.C. & Woolf, A.B. (2006). Postharvest quality of Dragon fruit (Hylocereus undatus) following disinfesting hot air treatments. Postharvest Biology and Technology, 41(1): 62-69.
  12. Ismail, N.S.M.; Ramli, N.; Hani, N.M. & Meon, Z. (2012). Extraction and characterization of pectin from dragon fruit (Hylocereus polyrhizus) using various extraction conditions. Sains Malaysiana, 41(1): 41-45.
  13. Jamilah, B.; Shu, C. E.; Kharidah, M.; Dzulkifly, M. A. & Noranizan, A. (2011). Physico-chemical characteristics of red pitaya (Hylocereus polyrhizus) peel. International Food Research Journal, 18: 279-286.
  14. Kalapathy, U. & Proctor, A. (2001). Effect of acid extraction and alcohol precipitation conditions on the yield and purity of soy hull pectin. Food Chemistry, 73: 393-396.
  15. Le Bellec, F.; Vaillant, F. & Imbert, E. (2006). Pitahaya (Hylocereus spp.): A new fruit crop, a market with a future. Fruits, 61: 237-250.
  16. Levigne, S.; Ralet, M.C. & Thibault, J.F. (2002). Characteriation of pectin extracted from fresh sugar beet under different conditions using an experimental design. Carbohydrate Polymer, 49: 145-153.
  17. Liu, Y.; Shi, J. & Langrish, T.A.G. (2006). Water-based extraction of pectin from flavedo and albedo of orange peels. Chemical Engineering Journal, 120: 203-209.
  18. Mahattanatawee, K.; Manthey, J.A.; Luzio, G.; Talcott, S.T ; Goodner, K. & Baldwin,
  19. E.A. (2006).Total antioxidant activity and fiber content of select Florida-grown tropical fruits. J. Agric. Food Chem., 54: 7355-7363.
  20. McCready, R.M. (1970). Pectin: Pp: 565-595. In Joslyn, M.A. (Ed.). Methods in Food Analysis, Physical, Chemical and Instrumental Methods of Analysis. New York. Academic Press: 845pp.
  21. Mizrahi, Y.; Nerd, A. & Nobel, P.S. (1997). Cacti as crops. Horticulture Reviews, 18: 291-319.
  22. Mohamed, S. & Hasan, Z. (1995). Extraction and characterization of pectin from various tropical agcowastes. Asian Food Journal, 10: 43-50.
  23. Nerd, A.; Sitrita, Y.; Kaushika, R.A. & Mizrahi, Y. (2002). High summer temperatures inhibit flowering in vine pitaya crops (Hylocereus spp.). Scientia Horticulture, 96(1): 343-350.
  24. Rahmati, S.; Abdullah, A.; Momeny, E. & Kang, O.L. (2015). Optimization studies on microwave assisted extraction of dragon fruit (Hylocereus polyrhizus) peel pectin using response surface methodology. International Food Research Journal, 22(1): 233-239.
  25. Ramli, N. & Asmawati, M.S. (2011). Effect of ammonium oxalate and acetic acid at several extraction time and pH on some physicochemical properties of pectin from cocoa husk (Theobroma cacao). African Journal of Food Science, 5: 790 -798.
  26. Ranganna, S. (2008). Handbook of Analysis and Quality Control for Fruits and Vegetable Products 15th ed. New Delhi: McGraw Hill Publishing Co. Ltd.: 1112pp.
  27. Redgwell, R.J.; MacRae, E.; Hallett, I.; Fischer, M.; Perry, J. & Harker, R. (1997). In vivo and in vitro swelling of cell walls during fruit ripening. Planta, 203: 162-173.
  28. Sakai, T.; Sakamoto, T.; Hallacrt, J. & Vandamme, E.C. (1993). Pectin, pectinase and proto pectin: Production properties and application. Advance in Applied Microbiology, 39: 213-218.
  29. Shaha, R.K.; Nayagl, Y.; Punichelvana, A.P. & Afandi, A. (2013). Optimized extraction condition and characterization of pectin from kaffir lime (Citrus hystrix). Research Journal of Agriculture and Forestry Sciences, 1(2): 1-11.
  30. Singthong, J.; Cui, S.W.; Ningsanond, S. & Douglas Goff, H. (2004). Structural characterization, degree of esterification and some gelling properties of Krueo Ma Noy (Cissampelos pareira) pectin. Carbohydrate Polymers, 58(4): 391-400.
  31. Sirisakulwat, S.; Nagel, A.; Sruamsiri, P.; Carle, R. & Neidhart S. (2008). Yield and quality of pectin extractable from the peels of Thai mango cultivars depending on fruit ripeness. J. Agricult. Food Chem., 56: 10727-10738.
  32. Sundar Raj, A.A; Rubila, S.; Jayabalan, R. & Ranganathan, T.V. (2012). A review on pectin: Chemistry due to general properties of pectin and pharmaceutical uses. Scientific Reports, 1(2): 1-4.
  33. Tsoga, A.; Richardson, R.K. & Morris, E.R. (2004). Role of cosolutes in gelation of high methoxy pectin. Part 1. Comparison of sugars and polyols. Food Hydrocolloids, 18(6): 907-919.
  34. Yeoh, S.; Shi, J. & Langrish, T.A.G. (2008). Comparisons between different techniques for water-based extraction of pectin from orange peels. Desalination, 218: 229-237.
  35. Yoo, S.H.; Fishman, M.L.; Hotchkiss, A.T. & Lee, H.G. (2006). Viscometric behavior of high-methoxyl and lwo-methoxyl pectin solution. Food Hydrocolloids, 20: 62-67.
  36. Zhang, C. & Taihua, M.U. (2011). Optimisation of pectin extraction from sweet potato (Ipomoea batatas, Convolvulaceae) residues with disodium phosphate solution by response surface method. International Journal of Food Science and Technology, 46(11): 2274-